CCRIS 6706

Name	1,2,3-Tribromopropane
Synonyms	NSC 78932 AI3-18135 CCRIS 6706 BRN 1732082 s-Tribromopropane sym-Tribromopropane 1,2,3-Tribromopropane 1,2,3-tribromo-propan glyceryltribromohydrin GLYCEROL TRIBROMOHYDRIN propane,1,2,3-tribromo- Glycerol tribromohydrin Glyceryl tribromohydrin Propane, 1,2,3-tribromo- 4-01-00-00221 (Beilstein Handbook Reference)
CAS	96-11-7
EINECS	202-478-8
InChI	InChI=1/C3H5Br3/c4-1-3(6)2-5/h3H,1-2H2

Molecular Formula	C3H5Br3
Molar Mass	280.78
Density	2.398g/mLat 25°C(lit.)
Melting Point	16-17°C(lit.)
Boling Point	220°C(lit.)
Flash Point	200°F
Solubility	H2O: insoluble
Vapor Presure	0.167mmHg at 25°C
Merck	14,9614
BRN	1732082
Storage Condition	Store below +30°C.
Refractive Index	n20/D 1.584(lit.)
Physical and Chemical Properties	Boiling Point: 220 Melting Point: 16 - 17 density: 2.398

Hazard Symbols	Xn - Harmful
Risk Codes	R20/21/22 - Harmful by inhalation, in contact with skin and if swallowed. R36/37/38 - Irritating to eyes, respiratory system and skin. R40 - Limited evidence of a carcinogenic effect R68 - Possible risk of irreversible effects
Safety Description	S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S27 - Take off immediately all contaminated clothing. S36/37/39 - Wear suitable protective clothing, gloves and eye/face protection.
UN IDs	2810
WGK Germany	3
RTECS	TZ8300000
TSCA	Yes
HS Code	2903 39 19
Hazard Class	6.1(b)
Packing Group	II

NIST chemical information	information provided by: webbook.nist.gov (external link)
EPA chemical substance information	information provided by: ofmpeb.epa.gov (external link)
production method	1. Preparation Method: In the reaction bottle equipped with stirrer, reflux condenser (equipped with calcium chloride drying tube), dropping funnel, thermometer, add allyl bromide (2)182g(1.5mol), ML of dried carbon tetrachloride. The ice-salt bath was cooled to -5 ° C., and 255g(1.6mol) of dry bromine was added dropwise through a dropping funnel. The dropping acceleration was controlled so that the reaction solution rose to 0 ° C., and the addition was completed for about 1.5h. Slowly up to room temperature and continue to stir the reaction for 30min. The solvent was distilled under reduced pressure, and then a fraction of 92 to 93 ° C./1.33KPA was collected to obtain 400g of 1,2, 3-tribromopropane (1) as an almost colorless liquid in a yield of 95%. Note: (1) The allyl bromide is preferably treated before use, and the treatment method is as follows: first, dry with anhydrous calcium chloride, and then carry out distillation, and collect the fraction of 69~72 °c. [1]

Last Update：2024-04-10 22:29:15

Product Name: 1,2,3-Tribromopropane Request for quotation
CAS: 96-11-7
Tel: +86-21-56795779
Email: charles7788@worldyachem.com
Mobile: +86-13651600618
QQ: 2850607228

Wechat: 13651600618
WhatsApp: +8613651600618

Product Name: 1,2,3-Tribromopropane Request for quotation
CAS: 96-11-7
Tel: +86-21-56795779
Email: charles7788@worldyachem.com
Mobile: +86-13651600618
QQ: 2850607228

Wechat: 13651600618
WhatsApp: +8613651600618

View History

CCRIS 6706

CCRIS 6706 Request for Quotation